In-situ Raman spectroscopy studies of room-temperature and hydrothermal reactions

Brendan T. McGrail, Laurent J. Jouffret, Eric Villa, Peter C. Burns

Research output: Chapter in Book/Report/Conference proceedingConference contribution

1 Citation (Scopus)

Abstract

By contracting with the Parr Instrument Company and Bruker Optical Systems, we have developed a system for continuous monitoring of hydrothermal and room temperature reactions by Raman spectroscopy. Using the uranyl peroxide cage cluster {[UO2(O2)(OH)]16[UO2(O 2)2]4}24- (denoted {U 20R}) and a coordination polymer made from uranyl ions and 4,4′-biphenyldicarboxylate as model systems, we demonstrate the spectroscopically observable changes associated with reaction progress and crystallization.

Original languageEnglish
Title of host publicationActinides and Nuclear Energy Materials
Pages281-288
Number of pages8
Volume1444
DOIs
StatePublished - 2012
Externally publishedYes
Event2012 MRS Spring Meeting - San Francisco, CA, United States
Duration: Apr 9 2012Apr 13 2012

Other

Other2012 MRS Spring Meeting
CountryUnited States
CitySan Francisco, CA
Period4/9/124/13/12

Fingerprint

Peroxides
Crystallization
Optical systems
Raman spectroscopy
Polymers
Ions
Monitoring
peroxides
room temperature
coordination polymers
Industry
crystallization
Temperature
ions
temperature

All Science Journal Classification (ASJC) codes

  • Materials Science(all)
  • Condensed Matter Physics
  • Mechanical Engineering
  • Mechanics of Materials

Cite this

McGrail, B. T., Jouffret, L. J., Villa, E., & Burns, P. C. (2012). In-situ Raman spectroscopy studies of room-temperature and hydrothermal reactions. In Actinides and Nuclear Energy Materials (Vol. 1444, pp. 281-288) https://doi.org/10.1557/opl.2012.1127

In-situ Raman spectroscopy studies of room-temperature and hydrothermal reactions. / McGrail, Brendan T.; Jouffret, Laurent J.; Villa, Eric; Burns, Peter C.

Actinides and Nuclear Energy Materials. Vol. 1444 2012. p. 281-288.

Research output: Chapter in Book/Report/Conference proceedingConference contribution

McGrail, BT, Jouffret, LJ, Villa, E & Burns, PC 2012, In-situ Raman spectroscopy studies of room-temperature and hydrothermal reactions. in Actinides and Nuclear Energy Materials. vol. 1444, pp. 281-288, 2012 MRS Spring Meeting, San Francisco, CA, United States, 4/9/12. https://doi.org/10.1557/opl.2012.1127
McGrail BT, Jouffret LJ, Villa E, Burns PC. In-situ Raman spectroscopy studies of room-temperature and hydrothermal reactions. In Actinides and Nuclear Energy Materials. Vol. 1444. 2012. p. 281-288 https://doi.org/10.1557/opl.2012.1127
McGrail, Brendan T. ; Jouffret, Laurent J. ; Villa, Eric ; Burns, Peter C. / In-situ Raman spectroscopy studies of room-temperature and hydrothermal reactions. Actinides and Nuclear Energy Materials. Vol. 1444 2012. pp. 281-288
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