Abstract
By contracting with the Parr Instrument Company and Bruker Optical Systems, we have developed a system for continuous monitoring of hydrothermal and room temperature reactions by Raman spectroscopy. Using the uranyl peroxide cage cluster {[UO2(O2)(OH)]16[UO2(O 2)2]4}24- (denoted {U 20R}) and a coordination polymer made from uranyl ions and 4,4′-biphenyldicarboxylate as model systems, we demonstrate the spectroscopically observable changes associated with reaction progress and crystallization.
| Original language | English |
|---|---|
| Title of host publication | Actinides and Nuclear Energy Materials |
| Pages | 281-288 |
| Number of pages | 8 |
| Volume | 1444 |
| DOIs | |
| State | Published - 2012 |
| Externally published | Yes |
| Event | 2012 MRS Spring Meeting - San Francisco, CA, United States Duration: Apr 9 2012 → Apr 13 2012 |
Other
| Other | 2012 MRS Spring Meeting |
|---|---|
| Country | United States |
| City | San Francisco, CA |
| Period | 4/9/12 → 4/13/12 |
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All Science Journal Classification (ASJC) codes
- Materials Science(all)
- Condensed Matter Physics
- Mechanical Engineering
- Mechanics of Materials
Cite this
In-situ Raman spectroscopy studies of room-temperature and hydrothermal reactions. / McGrail, Brendan T.; Jouffret, Laurent J.; Villa, Eric; Burns, Peter C.
Actinides and Nuclear Energy Materials. Vol. 1444 2012. p. 281-288.Research output: Chapter in Book/Report/Conference proceeding › Conference contribution
}
TY - GEN
T1 - In-situ Raman spectroscopy studies of room-temperature and hydrothermal reactions
AU - McGrail, Brendan T.
AU - Jouffret, Laurent J.
AU - Villa, Eric
AU - Burns, Peter C.
PY - 2012
Y1 - 2012
N2 - By contracting with the Parr Instrument Company and Bruker Optical Systems, we have developed a system for continuous monitoring of hydrothermal and room temperature reactions by Raman spectroscopy. Using the uranyl peroxide cage cluster {[UO2(O2)(OH)]16[UO2(O 2)2]4}24- (denoted {U 20R}) and a coordination polymer made from uranyl ions and 4,4′-biphenyldicarboxylate as model systems, we demonstrate the spectroscopically observable changes associated with reaction progress and crystallization.
AB - By contracting with the Parr Instrument Company and Bruker Optical Systems, we have developed a system for continuous monitoring of hydrothermal and room temperature reactions by Raman spectroscopy. Using the uranyl peroxide cage cluster {[UO2(O2)(OH)]16[UO2(O 2)2]4}24- (denoted {U 20R}) and a coordination polymer made from uranyl ions and 4,4′-biphenyldicarboxylate as model systems, we demonstrate the spectroscopically observable changes associated with reaction progress and crystallization.
UR - http://www.scopus.com/inward/record.url?scp=84875510384&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=84875510384&partnerID=8YFLogxK
U2 - 10.1557/opl.2012.1127
DO - 10.1557/opl.2012.1127
M3 - Conference contribution
AN - SCOPUS:84875510384
SN - 9781605114217
VL - 1444
SP - 281
EP - 288
BT - Actinides and Nuclear Energy Materials
ER -