TY - JOUR
T1 - Synthesis and Characterization of Copper Complexes with a Tridentate Nitrogen-Donor Ligand
T2 - An Integrated Research Experiment for Undergraduate Students
AU - Bussey, Katherine A.
AU - Cavalier, Annie R.
AU - Connell, Jennifer R.
AU - Mraz, Margaret E.
AU - Holderread, Ashley S.
AU - Oshin, Kayode D.
AU - Pintauer, Tomislav
N1 - Publisher Copyright:
© 2015 The American Chemical Society and Division of Chemical Education, Inc.
PY - 2015/10/9
Y1 - 2015/10/9
N2 - An integrated laboratory experiment applying concepts and techniques developed in organic chemistry, inorganic chemistry, and instrumental analysis is presented for use by students interested in undergraduate research. The experiment incorporates some advanced laboratory practices such as multistep organic synthesis and purification, detailed reaction mechanism, air-sensitive metalation techniques, variable-temperature NMR experiments, cyclic voltammetry, and single crystal X-ray crystallography. Subsequently, students are presented with an experience that mirrors fundamental inorganic chemistry research practices found in laboratories throughout the world.
AB - An integrated laboratory experiment applying concepts and techniques developed in organic chemistry, inorganic chemistry, and instrumental analysis is presented for use by students interested in undergraduate research. The experiment incorporates some advanced laboratory practices such as multistep organic synthesis and purification, detailed reaction mechanism, air-sensitive metalation techniques, variable-temperature NMR experiments, cyclic voltammetry, and single crystal X-ray crystallography. Subsequently, students are presented with an experience that mirrors fundamental inorganic chemistry research practices found in laboratories throughout the world.
UR - http://www.scopus.com/inward/record.url?scp=84949035025&partnerID=8YFLogxK
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U2 - 10.1021/acs.jchemed.5b00175
DO - 10.1021/acs.jchemed.5b00175
M3 - Article
AN - SCOPUS:84949035025
VL - 92
SP - 2140
EP - 2145
JO - Journal of Chemical Education
JF - Journal of Chemical Education
SN - 0021-9584
IS - 12
ER -