Abstract
An integrated laboratory experiment applying concepts and techniques from organic chemistry, inorganic chemistry, and instrumental analysis is presented for use in the undergraduate curriculum. This experiment highlights the synthesis, characterization, and use of tris(2-pyridylmethyl)amine (TPMA) to make complexes with different metal salts. It incorporates laboratory practices such as literature searches, multistep synthesis, reaction mechanisms, NMR spectroscopy, and X-ray crystallography.
| Original language | English (US) |
|---|---|
| Pages (from-to) | 876-881 |
| Number of pages | 6 |
| Journal | Journal of Chemical Education |
| Volume | 95 |
| Issue number | 5 |
| DOIs | |
| State | Published - May 8 2018 |
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All Science Journal Classification (ASJC) codes
- Chemistry(all)
- Education
Cite this
X-ray Crystallography Analysis of Complexes Synthesized with Tris(2-pyridylmethyl)amine : A Laboratory Experiment for Undergraduate Students Integrating Interdisciplinary Concepts and Techniques. / Bazley, Isabel J.; Erie, Ellen A.; Feiereisel, Garrett M.; Lewarne, Christopher J.; Peterson, Jack M.; Sandquist, Katherine L.; Oshin, Kayode; Zeller, Matthias.
In: Journal of Chemical Education, Vol. 95, No. 5, 08.05.2018, p. 876-881.Research output: Contribution to journal › Article
}
TY - JOUR
T1 - X-ray Crystallography Analysis of Complexes Synthesized with Tris(2-pyridylmethyl)amine
T2 - A Laboratory Experiment for Undergraduate Students Integrating Interdisciplinary Concepts and Techniques
AU - Bazley, Isabel J.
AU - Erie, Ellen A.
AU - Feiereisel, Garrett M.
AU - Lewarne, Christopher J.
AU - Peterson, Jack M.
AU - Sandquist, Katherine L.
AU - Oshin, Kayode
AU - Zeller, Matthias
PY - 2018/5/8
Y1 - 2018/5/8
N2 - An integrated laboratory experiment applying concepts and techniques from organic chemistry, inorganic chemistry, and instrumental analysis is presented for use in the undergraduate curriculum. This experiment highlights the synthesis, characterization, and use of tris(2-pyridylmethyl)amine (TPMA) to make complexes with different metal salts. It incorporates laboratory practices such as literature searches, multistep synthesis, reaction mechanisms, NMR spectroscopy, and X-ray crystallography.
AB - An integrated laboratory experiment applying concepts and techniques from organic chemistry, inorganic chemistry, and instrumental analysis is presented for use in the undergraduate curriculum. This experiment highlights the synthesis, characterization, and use of tris(2-pyridylmethyl)amine (TPMA) to make complexes with different metal salts. It incorporates laboratory practices such as literature searches, multistep synthesis, reaction mechanisms, NMR spectroscopy, and X-ray crystallography.
UR - http://www.scopus.com/inward/record.url?scp=85046796954&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=85046796954&partnerID=8YFLogxK
U2 - 10.1021/acs.jchemed.7b00685
DO - 10.1021/acs.jchemed.7b00685
M3 - Article
VL - 95
SP - 876
EP - 881
JO - Journal of Chemical Education
JF - Journal of Chemical Education
SN - 0021-9584
IS - 5
ER -