TY - JOUR
T1 - X-ray Crystallography Analysis of Complexes Synthesized with Tris(2-pyridylmethyl)amine
T2 - A Laboratory Experiment for Undergraduate Students Integrating Interdisciplinary Concepts and Techniques
AU - Bazley, Isabel J.
AU - Erie, Ellen A.
AU - Feiereisel, Garrett M.
AU - Lewarne, Christopher J.
AU - Peterson, Jack M.
AU - Sandquist, Katherine L.
AU - Oshin, Kayode
AU - Zeller, Matthias
PY - 2018/5/8
Y1 - 2018/5/8
N2 - An integrated laboratory experiment applying concepts and techniques from organic chemistry, inorganic chemistry, and instrumental analysis is presented for use in the undergraduate curriculum. This experiment highlights the synthesis, characterization, and use of tris(2-pyridylmethyl)amine (TPMA) to make complexes with different metal salts. It incorporates laboratory practices such as literature searches, multistep synthesis, reaction mechanisms, NMR spectroscopy, and X-ray crystallography.
AB - An integrated laboratory experiment applying concepts and techniques from organic chemistry, inorganic chemistry, and instrumental analysis is presented for use in the undergraduate curriculum. This experiment highlights the synthesis, characterization, and use of tris(2-pyridylmethyl)amine (TPMA) to make complexes with different metal salts. It incorporates laboratory practices such as literature searches, multistep synthesis, reaction mechanisms, NMR spectroscopy, and X-ray crystallography.
UR - http://www.scopus.com/inward/record.url?scp=85046796954&partnerID=8YFLogxK
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U2 - 10.1021/acs.jchemed.7b00685
DO - 10.1021/acs.jchemed.7b00685
M3 - Article
AN - SCOPUS:85046796954
VL - 95
SP - 876
EP - 881
JO - Journal of Chemical Education
JF - Journal of Chemical Education
SN - 0021-9584
IS - 5
ER -