X-ray Crystallography Analysis of Complexes Synthesized with Tris(2-pyridylmethyl)amine

A Laboratory Experiment for Undergraduate Students Integrating Interdisciplinary Concepts and Techniques

Isabel J. Bazley, Ellen A. Erie, Garrett M. Feiereisel, Christopher J. Lewarne, Jack M. Peterson, Katherine L. Sandquist, Kayode Oshin, Matthias Zeller

Research output: Contribution to journalArticle

Abstract

An integrated laboratory experiment applying concepts and techniques from organic chemistry, inorganic chemistry, and instrumental analysis is presented for use in the undergraduate curriculum. This experiment highlights the synthesis, characterization, and use of tris(2-pyridylmethyl)amine (TPMA) to make complexes with different metal salts. It incorporates laboratory practices such as literature searches, multistep synthesis, reaction mechanisms, NMR spectroscopy, and X-ray crystallography.

Original languageEnglish (US)
Pages (from-to)876-881
Number of pages6
JournalJournal of Chemical Education
Volume95
Issue number5
DOIs
StatePublished - May 8 2018

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X ray crystallography
laboratory experiment
chemistry
Students
Curricula
Nuclear magnetic resonance spectroscopy
Salts
student
Metals
Experiments
curriculum
experiment
tris(2-pyridylmethyl)amine
Inorganic Chemistry
Organic Chemistry
literature

All Science Journal Classification (ASJC) codes

  • Chemistry(all)
  • Education

Cite this

X-ray Crystallography Analysis of Complexes Synthesized with Tris(2-pyridylmethyl)amine : A Laboratory Experiment for Undergraduate Students Integrating Interdisciplinary Concepts and Techniques. / Bazley, Isabel J.; Erie, Ellen A.; Feiereisel, Garrett M.; Lewarne, Christopher J.; Peterson, Jack M.; Sandquist, Katherine L.; Oshin, Kayode; Zeller, Matthias.

In: Journal of Chemical Education, Vol. 95, No. 5, 08.05.2018, p. 876-881.

Research output: Contribution to journalArticle

Bazley, Isabel J. ; Erie, Ellen A. ; Feiereisel, Garrett M. ; Lewarne, Christopher J. ; Peterson, Jack M. ; Sandquist, Katherine L. ; Oshin, Kayode ; Zeller, Matthias. / X-ray Crystallography Analysis of Complexes Synthesized with Tris(2-pyridylmethyl)amine : A Laboratory Experiment for Undergraduate Students Integrating Interdisciplinary Concepts and Techniques. In: Journal of Chemical Education. 2018 ; Vol. 95, No. 5. pp. 876-881.
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