X-ray Crystallography Analysis of Complexes Synthesized with Tris(2-pyridylmethyl)amine: A Laboratory Experiment for Undergraduate Students Integrating Interdisciplinary Concepts and Techniques

Isabel J. Bazley; Ellen A. Erie; Garrett M. Feiereisel; Christopher J. Lewarne; Jack M. Peterson; Katherine L. Sandquist; Kayode D. Oshin; Matthias Zeller

doi:10.1021/acs.jchemed.7b00685

X-ray Crystallography Analysis of Complexes Synthesized with Tris(2-pyridylmethyl)amine: A Laboratory Experiment for Undergraduate Students Integrating Interdisciplinary Concepts and Techniques

Isabel J. Bazley, Ellen A. Erie, Garrett M. Feiereisel, Christopher J. Lewarne, Jack M. Peterson, Katherine L. Sandquist, Kayode D. Oshin, Matthias Zeller

Department of Chemistry

Research output: Contribution to journal › Article › peer-review

5 Scopus citations

Abstract

An integrated laboratory experiment applying concepts and techniques from organic chemistry, inorganic chemistry, and instrumental analysis is presented for use in the undergraduate curriculum. This experiment highlights the synthesis, characterization, and use of tris(2-pyridylmethyl)amine (TPMA) to make complexes with different metal salts. It incorporates laboratory practices such as literature searches, multistep synthesis, reaction mechanisms, NMR spectroscopy, and X-ray crystallography.

Original language	English (US)
Pages (from-to)	876-881
Number of pages	6
Journal	Journal of chemical education
Volume	95
Issue number	5
DOIs	https://doi.org/10.1021/acs.jchemed.7b00685
State	Published - May 8 2018

All Science Journal Classification (ASJC) codes

Chemistry(all)
Education

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10.1021/acs.jchemed.7b00685

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Bazley, I. J., Erie, E. A., Feiereisel, G. M., Lewarne, C. J., Peterson, J. M., Sandquist, K. L., Oshin, K. D., & Zeller, M. (2018). X-ray Crystallography Analysis of Complexes Synthesized with Tris(2-pyridylmethyl)amine: A Laboratory Experiment for Undergraduate Students Integrating Interdisciplinary Concepts and Techniques. Journal of chemical education, 95(5), 876-881. https://doi.org/10.1021/acs.jchemed.7b00685

X-ray Crystallography Analysis of Complexes Synthesized with Tris(2-pyridylmethyl)amine : A Laboratory Experiment for Undergraduate Students Integrating Interdisciplinary Concepts and Techniques. / Bazley, Isabel J.; Erie, Ellen A.; Feiereisel, Garrett M.; Lewarne, Christopher J.; Peterson, Jack M.; Sandquist, Katherine L.; Oshin, Kayode D.; Zeller, Matthias.

In: Journal of chemical education, Vol. 95, No. 5, 08.05.2018, p. 876-881.

Research output: Contribution to journal › Article › peer-review

Bazley, IJ, Erie, EA, Feiereisel, GM, Lewarne, CJ, Peterson, JM, Sandquist, KL, Oshin, KD & Zeller, M 2018, 'X-ray Crystallography Analysis of Complexes Synthesized with Tris(2-pyridylmethyl)amine: A Laboratory Experiment for Undergraduate Students Integrating Interdisciplinary Concepts and Techniques', Journal of chemical education, vol. 95, no. 5, pp. 876-881. https://doi.org/10.1021/acs.jchemed.7b00685

Bazley IJ, Erie EA, Feiereisel GM, Lewarne CJ, Peterson JM, Sandquist KL et al. X-ray Crystallography Analysis of Complexes Synthesized with Tris(2-pyridylmethyl)amine: A Laboratory Experiment for Undergraduate Students Integrating Interdisciplinary Concepts and Techniques. Journal of chemical education. 2018 May 8;95(5):876-881. https://doi.org/10.1021/acs.jchemed.7b00685

Bazley, Isabel J. ; Erie, Ellen A. ; Feiereisel, Garrett M. ; Lewarne, Christopher J. ; Peterson, Jack M. ; Sandquist, Katherine L. ; Oshin, Kayode D. ; Zeller, Matthias. / X-ray Crystallography Analysis of Complexes Synthesized with Tris(2-pyridylmethyl)amine : A Laboratory Experiment for Undergraduate Students Integrating Interdisciplinary Concepts and Techniques. In: Journal of chemical education. 2018 ; Vol. 95, No. 5. pp. 876-881.

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abstract = "An integrated laboratory experiment applying concepts and techniques from organic chemistry, inorganic chemistry, and instrumental analysis is presented for use in the undergraduate curriculum. This experiment highlights the synthesis, characterization, and use of tris(2-pyridylmethyl)amine (TPMA) to make complexes with different metal salts. It incorporates laboratory practices such as literature searches, multistep synthesis, reaction mechanisms, NMR spectroscopy, and X-ray crystallography.",

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note = "Funding Information: The corresponding author would like to thank Creighton University and Purdue University for instrumentation support. This work is also supported by the National Science Foundation through the Major Research Instrumentation Program under Grant CHE-1625543. Funding Information: This work is also supported by the National Science Foundation through the Major Research Instrumentation Program under Grant CHE-1625543.",

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AU - Oshin, Kayode D.

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